The Gel Growth Technique—A Neglected Yet Effective Tool to Prepare Crystals of Oxysalts and Supergene Minerals

Abstract

The technique of crystal growth in gels has nowadays become somewhat neglected in the scope of earth sciences, to the disadvantage of the experimental mineralogist. Even preparing an inorganic silica gel can prove a challenge to many, let alone successfully configure the entire experiment. Based not only on previous literature but also on our extensive experience, crystals of many substances, including supergene minerals as reference standards, can be successfully grown in gel, aiding in accomplishing various research goals in earth sciences. Instead of providing the reader with an overwhelming compendium of historical information and theoretical knowledge of the subject which can be found elsewhere, we presented herein a comprehensive, practically oriented guide to the understanding and successful use of the technique of crystal growth in gels, mentioning, in addition to the general principle, the numerous pitfalls which we encountered during our own use of the method, and the ways to overcome them. Despite that the procedure is nowadays used mainly for the laboratory synthesis of organic or metal‐organic compounds, we believe it to be a valuable asset to any mineralogist, and often, the only way to obtain inorganic reference material of a particular mineral of interest.