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Iridium-catalyzed asymmetric hydrogenation of dibenzo[b,f][1,4]thiazepines

Pure and Applied Chemistry (2013) 85(4) 843-849
DOI: 10.1351/PAC-CON-12-07-02
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Abstract

Highly enantioselective hydrogenation of substituted dibenzo[b,f][1,4]thiazepines was achieved with up to 96 % ee (enantiomeric excess) using [Ir(COD)Cl]2/(R)-SynPhos complex as catalyst in the presence of iodine. This method provides an efficient access to optically active 11-substituted-10,11-dihydrodibenzo[b,f][1,4]thiazepines. © 2013 IUPAC.

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Guo, R. N., Gao, K., Ye, Z. S., Shi, L., Li, Y., & Zhou, Y. G. (2013). Iridium-catalyzed asymmetric hydrogenation of dibenzo[b,f][1,4]thiazepines. Pure and Applied Chemistry, 85(4), 843–849. https://doi.org/10.1351/PAC-CON-12-07-02

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