Abstract
Acylation of the readily available 3-methyl-3-hydroxymethyl oxetane (2) leads to the corresponding oxetane esters (3) which rearrange smoothly in the presence of boron trifluoride etherate in methylene chloride at -15° to form ortho esters of the 2, 6, 7-trioxabicyclo[2.2.2]octane series (4). © 1983.
Cite
CITATION STYLE
APA
Corey, E. J., & Raju, N. (1983). A new general synthetic route to bridged carboxylic ortho esters. Tetrahedron Letters, 24(50), 5571–5574. https://doi.org/10.1016/S0040-4039(00)94143-1
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