Measurement of elastic properties of brittle materials by ultrasonic and indentation methods

Abstract

The measurements of acoustic properties of three brittle materials i.e., ITO (alkaline earth boro-aluminosilicate) glass, bulk metallic glass (BMG) and nickel-based superalloy (CM247LC) are conducted in this work to obtain various properties. The elastic moduli of materials are derived from the results by simple acoustic speed-elasticity relationship and compared with the data obtained with nanoindentation. The difference between the Young's modulus of ITO glass by ultrasonic and nanoindentation is 0.83%, a perfect match within range error. As for BMG, the difference (Young's modulus) is 23.59%, and 5.11% for the CM247LC superalloys. The pulse-echo method proves to be reliable for homogeneous amorphous glass, however, the elastic moduli of metallic glass and CM247LC superalloy by ultrasonic are quite different from those by nanoindentation. The difference is large enough to cover the maximal error associated with the nanoindentation method. The relationship of acoustic speed and elastic constants must be reviewed in dealing with compound materials.