One Pot Synthesis and Characterization of Palladium [Pd(Anil-Tolu)4(H2O)2]by insitu Method

Abstract

The insitu synthesis of Schiff base metal complex using p-toluedine (p-tolu), p-anisaldehyde (p-anisal) as starting materials with Palladium nitrate hexahydrate (Pd(NO3)2.6H2O) as a metal precursor in the molar ratio (1:1:1 M) at room temperature. The prepared metal complex is washed with several times with ethanol and boiled water for the removal of un-reacted materials completely. To confirm the prepared material by the following characterization like UV-visible spectroscopy, Fourier Transforms Infrared spectroscopy, X-ray diffraction pattern and Cyclic Voltammetry.