Abstract
A practical synthesis of 1,2,3,4,5,6-hexahydro-1,5-imino-10-hydroxy-9-methoxy-3,8,11-trimethyl-3-benza zocin-4-one (3) as an ABC ring model compound of ecteinascidin 743 and safracins from 3-hydroxy-4-methoxy-5-methylbenzaldehyde (7) is described. The overall yield in 15 step is 27%.
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Saito, N., Tachi, M., Seki, R. I., Kamayachi, H., & Kubo, A. (2000). A practical synthesis of the ABC ring model of ecteinascidins. Chemical and Pharmaceutical Bulletin, 48(10), 1549–1557. https://doi.org/10.1248/cpb.48.1549
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