Abstract
Molybdenum trichloride was successfully prepared in quantity b y the reduction of molybdenum p entachloridc with hydrogen. The most satisfactory yields were obLained with a 4 to 5 mole excess of hydrogen at pressures of 100 psi or higher and at a temp erature of 125°C. Molybdenum tetrachloride "'as prepared by direct reaction of mol ybde num trichloride with mol ybdenum pentachloride in a sealed tube or steel bomb maintained at 250 0 C. X-ray patterns of the various chlorides were obtained.
Cite
CITATION STYLE
Couch, D. E., & Brenner, A. (1959). Preparation of trichloride and tetrachloride of molybdenum. Journal of Research of the National Bureau of Standards Section A: Physics and Chemistry, 63A(2), 185. https://doi.org/10.6028/jres.063a.013
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