Effect of acidic primers on adhesive bonding of tri-n-butylborane initiated adhesive resin to alumina.

Abstract

The present study was conducted to evaluate the effect of acidic primers on adhesive bonding to sintered alumina. Alumina disk specimens were primed with one of the following acidic materials: Acryl Bond, All Bond II Primer B, Alloy Primer, Estenia Opaque Primer, Eye Sight Opaque Primer, M.L. Primer, MR. Bond, and Super-Bond Liquid. The disks were bonded with an adhesive resin (Super-Bond) initiated with a tri-n-butylborane (TBB) derivative, and bond strengths were determined. Average bond strength before thermocycling varied from 42.9 to 44.3 MPa, whereas post-thermocycling bond strength ranged from 22.0 to 42.8 MPa. Of the nine groups assessed, reduction of bond strength after thermocycling was not significant in three: Alloy Primer, Estenia Opaque Primer, and Eye Sight Opaque Primer. It can be concluded that phosphate-based primers are recommended for bonding sintered alumina with Super-Bond resin.