Crystal structure of 4-(2-hydroxy-3-methoxybenzylamino) benzoic acid dimethylformamide monosolvate monohydrate

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Abstract

The title compound, C15H15NO4·C3H7NO·H2O, a secondary amine molecule, is accompanied by one equivalent of water and one equivalent of dimethylformamide (DMF) as solvents. The molecule is non-planar, with a Caryl - CH2 - NH - Caryl torsion angle of -66.3(3)°. In the crystal, O - H⋯O and N - H⋯O hydrogen-bonding interactions between the amine molecules and the two types of solvent molecule result in the formation of a layered structure extending parallel to (010).

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Faizi, M. S. H., Kamaal, S., Ali, A., Ahmad, M., & Golenya, I. A. (2019). Crystal structure of 4-(2-hydroxy-3-methoxybenzylamino) benzoic acid dimethylformamide monosolvate monohydrate. Acta Crystallographica Section E: Crystallographic Communications, 75, 646–649. https://doi.org/10.1107/S2056989019005103

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