(R)-2,3,4,5-Tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine and rac-5-benzoyl-2,3,4,5-tetrahydro2,2,4-trimethyl-1,-5-benzothiazepine: Chains built from N - H⋯S and C - H⋯π(arene) hydrogen bonds

Manivannan Muthukumar; Kanagasabapathy Thanikasalam; E. Mothi Mohamed; John N. Low; Christopher Glidewell

Journal ArticleOPEN ACCESS

(R)-2,3,4,5-Tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine and rac-5-benzoyl-2,3,4,5-tetrahydro2,2,4-trimethyl-1,-5-benzothiazepine: Chains built from N - H⋯S and C - H⋯π(arene) hydrogen bonds

Acta Crystallographica Section C: Crystal Structure Communications (2004) 60(5)

DOI: 10.1107/S0108270104006857

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Abstract

Molecules of (K)-2,3,4,5-tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine. C12H17NS, are linked into spiral C(5) chains by a single N-H⋯S hydrogen bond, while molecules of rac-5-benzoyl-2,3,4,5-tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine, C 19H21NOS, are linked into zigzag chains by a C-H⋯π(arene) hydrogen bond.

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Muthukumar, M., Thanikasalam, K., Mohamed, E. M., Low, J. N., & Glidewell, C. (2004). (R)-2,3,4,5-Tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine and rac-5-benzoyl-2,3,4,5-tetrahydro2,2,4-trimethyl-1,-5-benzothiazepine: Chains built from N - H⋯S and C - H⋯π(arene) hydrogen bonds. Acta Crystallographica Section C: Crystal Structure Communications, 60(5). https://doi.org/10.1107/S0108270104006857

(R)-2,3,4,5-Tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine and rac-5-benzoyl-2,3,4,5-tetrahydro2,2,4-trimethyl-1,-5-benzothiazepine: Chains built from N - H⋯S and C - H⋯π(arene) hydrogen bonds

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