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A convenient synthesis and a NMR study of the diammoniate of diborane

Chemistry - A European Journal (2012) 18(12) 3490-3492
DOI: 10.1002/chem.201103693
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Abstract

DADB synthesis: The diammoniate of diborane (DADB) was synthesized in a new metathesis reaction between the diammoniate of monochloroborane and potassium borohydride in liquid ammonia (see scheme). 1H and 11B NMR spectra of DADB are reported. The stability in THF was examined by variable-temperature 11B NMR spectroscopy. Copyright © 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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Lingam, H. K., Chen, X., Zhao, J. C., & Shore, S. G. (2012). A convenient synthesis and a NMR study of the diammoniate of diborane. Chemistry - A European Journal, 18(12), 3490–3492. https://doi.org/10.1002/chem.201103693

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