Application of the crystalline sponge method to revise the structure of the phenalenone fuliginone

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Abstract

The structure of fuliginone was revised from a phenyl substituted phenalenone to a hydroxyl substituted phenalenone as a result of its re-purification via HPLC with subsequent NMR analysis together with an independent synthesis and analysis of the crystal structure, which was secured via the crystalline sponge method. On-flow High Performance Liquid Chromatography coupled to Nuclear Magnetic Resonance spectroscopy (HPLC-NMR) was employed to confirm the presence of the natural product in the plant extract and to monitor for any possible degradation or conversion of the compound.

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Brkljaca, R., Schneider, B., Hidalgo, W., Otálvaro, F., Ospina, F., Lee, S., … Urban, S. (2017). Application of the crystalline sponge method to revise the structure of the phenalenone fuliginone. Molecules, 22(2). https://doi.org/10.3390/molecules22020211

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