Abstract
Fibrous nanosilica (KCC-1) oxynitrides are promising solid-base catalysts. Paradoxically, when their nitrogen content increases, their catalytic activity decreases. This counterintuitive observation is explained here for the first time using 15N-solid-state NMR spectroscopy enhanced by dynamic nuclear polarization.
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Thankamony, A. S. L., Lion, C., Pourpoint, F., Singh, B., Linde, A. J. P., Carnevale, D., … Polshettiwar, V. (2015). Insights into the catalytic activity of nitridated fibrous silica (KCC-1) Nanocatalysts from 15 N and 29 Si NMR Spectroscopy Enhanced by Dynamic Nuclear Polarization. Angewandte Chemie - International Edition, 54(7), 2190–2193. https://doi.org/10.1002/anie.201406463
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