Effect of synthesis temperature, nucleation time, and postsynthesis heat treatment of ZnO nanoparticles and its sensing properties

Abstract

Control in size, crystallinity, and optical properties of ZnO nanoparticles (NPs) synthesized via coprecipitate method were investigated. A systematic change in particle size, crystallinity, and optical properties was observed by increasing synthesis temperature from 65°C to 75°C. A detailed study also suggested that smaller nucleation time is better to control the size distribution but the crystallinity will be compromised accordingly. Postannealing of ZnO NPs at 400°C also improves the crystal quality. Ultraviolet (UV) sensors were successfully synthesized and the results suggested that as-synthesized ZnO NPs can be used as active material for sensor applications.