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Easy preparation of [bis(trifluoroacetoxy)iodo]arenes from iodoarenes, with sodium percarbonate as the oxidant

Molecules (2002) 7(11) 810-812
DOI: 10.3390/71100810
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Abstract

Easy and effective preparations of the nearly pure [bis(trifluoroacetoxy) iodo]arenes, ArI(OCOCF)3, from some iodoarenes, ArI, are reported, using an anhydrous) sodium (percarbonate/(CF3CO)2O/CH 2Cl2 system. The colorless, freshly prepared (ArI(OCOCF)3)2 thus obtained were 98-99% pure (by iodometry).

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Kazmierczak, P., & Skulski, L. (2002). Easy preparation of [bis(trifluoroacetoxy)iodo]arenes from iodoarenes, with sodium percarbonate as the oxidant. In Molecules (Vol. 7, pp. 810–812). Molecular Diversity Preservation International. https://doi.org/10.3390/71100810

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