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Synthesis and characterization of ni(II) complex with 5,5,7,12,12,14-hexamethyl-1,4,8,11- Tetraazacyclotetradeca-7,14-dienium bromide

AIP Conference Proceedings (2014) 1614 358-361
DOI: 10.1063/1.4895222
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Abstract

Nickel(II) complex have been synthesized by treating a 14-membered ring tetraaza macrocyclic compound, 5,5,7,12,12,14- hexamethyl-1,4,8,11- Tetraazacyclotetradeca- 7,14- dienium, bromide (Me 6 N 4 H 4 )Br 2 with nickel acetate in metanol. The complex was characterized using elemental analysis, Fourier Transform Infrared (FTIR), Ultraviolet- Visible (UV-Vis), and single crystal diffraction (X-ray). The nickel atom coordinates through four nitrogen atoms in the ligand. Square planar geometry has been proposed for this complex.

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Yusoff, L. M., Yusoff, S. F. M., Ismail, W., & Yamin, B. M. (2014). Synthesis and characterization of ni(II) complex with 5,5,7,12,12,14-hexamethyl-1,4,8,11- Tetraazacyclotetradeca-7,14-dienium bromide. In AIP Conference Proceedings (Vol. 1614, pp. 358–361). American Institute of Physics Inc. https://doi.org/10.1063/1.4895222

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