The fabrication of fragrance microcapsules and their sustained and broken release behavior

Abstract

Their controlled release property is the most important feature of functional microcapsules and carriers. In this work, melamine resin shell fragrance microcapsules were fabricated in a non-ionic system, and their chemical structure, particle size, and morphology were analyzed. The sustained release property of the prepared microcapsules over 2400 h was studied with a weighing calculation method, and based on the fitting results, the release rate trend was consistent with the Peppas model (y = 100 - 2.30t 0.3213 ). Furthermore, the sustained and broken release behavior of the microcapsules in impregnated fabric samples were investigated for the first time by our proposed Solid Phase Microextraction-Gas Chromatography-Mass Spectrometer (SPME-GC-MS) method. The qualitative and quantitative analysis results showed that the middle and base note compositions were outstanding in the sustained release state, and the top note showed more advantages in the broken release state. In addition, it was found that the characteristic peak species and intensities of the sample finished with the microcapsules were more similar to pure essence oil than the sample finished by traditional methods, suggesting that the prepared microcapsules showed an excellent odor recovery and strength.