Studies toward the synthesis of azadirachtin, part 1: Total synthesis of a fully functionalized ABC ring framework and coupling with a norbornene domain

K. C. Nicolaou; Pradip K. Sasmal; A. J. Roecker; Xiao Wen Sun; Sunil Mandal; Antonella Converso

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Studies toward the synthesis of azadirachtin, part 1: Total synthesis of a fully functionalized ABC ring framework and coupling with a norbornene domain

Angewandte Chemie - International Edition (2005) 44(22) 3443-3447

DOI: 10.1002/anie.200500216

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Abstract

(Chemical Equation Presented) The advanced decalin intermediate 1 was synthesized and elaborated into the potential azadirachtin precursor 2. The challenging synthesis involved several protecting-group manipulations and coupling of 1 with an appropriate norbornene unit. © 2005 Wiley-VCH Verlag GmbH & Co. KGaA.

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Nicolaou, K. C., Sasmal, P. K., Roecker, A. J., Sun, X. W., Mandal, S., & Converso, A. (2005). Studies toward the synthesis of azadirachtin, part 1: Total synthesis of a fully functionalized ABC ring framework and coupling with a norbornene domain. Angewandte Chemie - International Edition, 44(22), 3443–3447. https://doi.org/10.1002/anie.200500216

Studies toward the synthesis of azadirachtin, part 1: Total synthesis of a fully functionalized ABC ring framework and coupling with a norbornene domain

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