Effect of glass fibers thermal treatment on the mechanical and thermal behavior of polysulfone based composites

Abstract

The effect of thermal treatment of glass fibers (GF) on the mechanical and thermo-mechanical properties of polysulfone (PSU) based composites reinforced with GF was investigated. Flexural and shear tests were used to study the composites' mechanical properties. A dynamic mechanical analysis (DMA) and a heat deflection temperature (HDT) test were used to study the thermo-mechanical properties of composites. The chemical structure of the composites was studied using IR-spectroscopy, and scanning electron microscopy (SEM) was used to illustrate the microstructure of the fracture surface. Three fiber to polymer ratios of initial and preheated GF composites (50/50, 60/40, 70/30 (wt. %) were studied. The results showed that the mechanical and thermo-mechanical properties improved with an increase in the fiber to polymer ratio. The interfacial adhesion in the preheated composites enhanced as a result of removing the sizing coating during the thermal treatment of GF, which improved the properties of the preheated composites compared with the composites reinforced with initial untreated fibers. The SEM images showed a good distribution of the polymer on the GF surface in the preheated GF composites.