Synthesis, separation and structure elucidation of a missing C60 chloride: C2v-C60Cl8

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Abstract

The so far missing chloro analog of the bromofullerene C 2v-C60Br8 has been synthesized by reaction of C60 fullerene with iodine monochloride. The title compound has been separated by means of HPLC, and its molecular structure has been unambiguously determined by single-crystal X-ray analysis. A facile synthesis of C s-C60Cl6 and C2v-C 60Cl8 in preparative amounts is presented. © 2012 Verlag der Zeitschrift fur Naturforschung.

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Ziegler, K., Amsharov, K. Y., & Jansen, M. (2012). Synthesis, separation and structure elucidation of a missing C60 chloride: C2v-C60Cl8. Zeitschrift Fur Naturforschung - Section B Journal of Chemical Sciences, 67(10), 1091–1097. https://doi.org/10.5560/ZNB.2012-0190

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