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A scalable, chromatography-free synthesis of benzotetramisole

Synthesis (Germany) (2014) 46(6)
DOI: 10.1055/s-0034-1378931
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Abstract

The scalable, chromatography-free synthesis of the chiral isothiourea benzotetramisole (BTM) in two steps from commercially available materials is presented. A detailed procedure for the synthesis of both enantiomers and the racemate on ca. 10 gram scale is disclosed.

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Daniels, D. S. B., Smith, S. R., Lebl, T., Shapland, P., & Smith, A. D. (2014). A scalable, chromatography-free synthesis of benzotetramisole. Synthesis (Germany), 46(6). https://doi.org/10.1055/s-0034-1378931

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