Optimization Using Central Composite Design of the Response Surface Methodology for the Compressive Strength of Alkali-Activated Material from Rice Husk Ash

Abstract

Alkali-activated materials are promising alternatives to cement. This study investigated the effects of the silica content, particle size, and replacement ratio of rice husk ash (RHA) on the compressive strength and the optimization of these parameters. Seventeen mixtures with different materials were tested to evaluate their compressive strengths. Three levels of particle size, silica content, and RHA replacement ratio were used. The effects of RHA characteristics on the compressive strength were investigated based on Archimedes porosity, pH, ignition loss, and X-ray diffraction. The experimental results reveal that the replacement ratio of RHA was p-values < 0.002, which affected the compressive strength compared with the particle size (p-values < 0.450) and silica content of the RHA (p-values < 0.017). It was confirmed that the optimum values of particle size, silica content, and replacement ratio of RHA were 50 µm, 90%, and 15 wt.%, respectively. After re-testing, the compressive strength of mortar made with the optimum values was 49.8 MPa. This increase in compressive strength was also found to be closely related to the porosity, pH, and ignition loss of the paste. It was confirmed that the replacement ratio of RHA increased with decreasing porosity and pH and increasing ignition loss, which was related to the formation of calcite and C-S-H.