Synthesis and microstructure evaluation of ODS steel 316L with zirconia dispersion

Abstract

An Austenitic ODS steel was developed for reactor structural material by dispersed 0.5 wt % of nano powder zirconia (ZrO2) to the AISI 316L steel. The synthesis was carried out by the powder metallurgy process with high energy milling and cooled compacting process. A new apparatus of APS (Arc Plasma Sintering) was used for consolidation the sample in the sintering process. Characterizations of the microstructure and elemental composition distribution were performed using the Scanning Electron Microscope (SEM) with X-ray Diffraction Spectroscopy (EDX) and area mapping. Identification for the change of phasesand hardness were analyzed using the XRD-test and Vickers Hardness measurement. Austenitic phase with relatively equiaxed grain and homogeny distribution of the ZrO2 dispersoid were identified after the sintering process followed by the improvement of hardness due to the pinning effect of the grain boundaries.