Transmission Bragg edge spectroscopy measurements at ORNL spallation neutron source

Abstract

Results of neutron transmission Bragg edge spectroscopic experiments performed at the SNAP beamline of the Spallation Neutron Source are presented. A high resolution neutron counting detector with a neutron sensitive microchannel plate and Timepix ASIC readout is capable of energy resolved two dimensional mapping of neutron transmission with spatial accuracy of ∼55 μm, limited by the readout pixel size, and energy resolution limited by the duration of the initial neutron pulse. A two dimensional map of the Fe 110 Bragg edge position was obtained for a bent steel screw sample. Although the neutron pulse duration corresponded to ∼30 mÅ energy resolution for 15.3 m flight path, the accuracy of the Bragg edge position in our measurements was improved by analytical fitting to a few mÅ level. A two dimensional strain map was calculated from measured Bragg edge values with an accuracy of ∼few hundreds μistrain for 300s of data acquisition time. © 2010 IOP Publishing Ltd.