Spectroscopic characterization of palm stearin biodiesel derived through base catalysed transesterification process

Abstract

In this research work, the characterization of the palm stearin biodiesel was made using Nuclear Magnetic resonance (NMR), Fourier transform infrared spectroscopy (FITR) and GC/MS methods. Analysis of the composition of fatty acids was done using the GCMS apparatus based on the retention time. Fourier transform infrared spectrometer was used for the spectrum analysis of the various functional groups and bands located in it. The properties of the palm stearin biodiesel were predicted adopting the American Society for Testing and Materials (ASTM) standards. Measured values of the properties were the density at 18°C as 0.88 g/m3, kinematic viscosity at 35°C as 3.4 mm2/s, the calorific value of the palm stearin as 37121 kJ/kg and the flash and fire points of the biodiesel as 130°C and 160oC respectively. The rapid and correct characterization of the palm stearin biodiesel was made by the NMR.