Clearing the undergrowth: detection and quantification of low level impurities using 19F NMR

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Abstract

A new method for the analysis of low level impurities in sparsely fluorinated species allows measurement of clean high dynamic range 19F spectra, fully decoupled and free of interfering signals from 13C isotopomers.

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Moutzouri, P., Kiraly, P., Phillips, A. R., Coombes, S. R., Nilsson, M., & Morris, G. A. (2017). Clearing the undergrowth: detection and quantification of low level impurities using 19F NMR. Chemical Communications, 53(1), 123–125. https://doi.org/10.1039/c6cc08836h

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