Synthesis and characterization of chromium oxide nanoparticles

Abstract

Chromium oxide nanoparticles (NPs) have been rapidly synthesized by precipitation method using ammomia as precipitating agent and are characterized by using X-ray Diffraction (XRD), Thermo Gravimetric Analysis (TGA), UV-Visible absorption (UV), Infrared Spectoscopy (IR), Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM). XRD studies show that chromium oxide NP is formed as Cr2 O3 and it has hexagonal structure. The shape and particle size of the synthesized Cr2O3 NPs is determined by SEM and TEM. The images showed that the size of NPs of Cr2O3 varied from 20 nm to 70 nm with average crystalline size 45 nm. UVVisible absorption and IR spectoscopy confirm the formation of nanosized Cr2O3 . TGA verifies that the Cr2O3 NPs are thermally stable upto 1000 ° C. Nanaoparticles chromium oxide TEM metal oxides XRD analysis.