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Tandem Baeyer–Villiger/Wittig/oxa-Michael addition: One-step to 5-substituted γ-lactones

Tetrahedron Letters (2023) 123
DOI: 10.1016/j.tetlet.2023.154545
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Abstract

The results reported in this study provide a practical protocol for the construction, in one single step of synthetically important γ-lactones in good yields starting from α‐hydroxy cyclobutanone, H2O2 and several stabilized phosphonium ylides. Our synthetic strategy relies on a tandem Baeyer–Villiger oxidation/Wittig reaction/oxa-Michael addition.

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Barranco, S., Cuccu, F., Caboni, P., & Frongia, A. (2023). Tandem Baeyer–Villiger/Wittig/oxa-Michael addition: One-step to 5-substituted γ-lactones. Tetrahedron Letters, 123. https://doi.org/10.1016/j.tetlet.2023.154545

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