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Synthesis and characterization of cationic tetramethyl tantalum(V) complex

Catalysts (2018) 8(11)
DOI: 10.3390/catal8110507
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Abstract

A novel method for the synthesis of the homogeneous homoleptic cationic tantalum(V)tetramethyl complex [(TaMe4)+ MeB(C6 F5)3−] from neutral tantalumpentamethyl (TaMe5) has been described, by direct demethylation using B(C6 F5)3 reagent. The aforesaid higher valent cationic tantalum complex was characterized precisely by liquid state1 H-NMR,13 C-NMR, and1 H-13 C-NMR correlation spectroscopy.

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Dey, R., Mohandas, J. C., Samantaray, M. K., Hamieh, A., Kavitake, S., Chen, Y., … Basset, J. M. (2018). Synthesis and characterization of cationic tetramethyl tantalum(V) complex. Catalysts, 8(11). https://doi.org/10.3390/catal8110507

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