Abstract
A wide range of anilines, benzylamines and some N-heterocyclics can be ortho-deuterated at room temperature using deuterium gas and cycloocta-1,5-dienyliridium(I)-1,1,1,5,5,5-hexafluoropentan-2,4-dionate in DMF or DMA. The method is applicable to labelling with tritium. Copyright © 2004 John Wiley & Sons, Ltd.
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Garman, R. N., Hickey, M. J., Kingston, L. P., McAuley, B., Jones, J. R., Lockley, W. J. S., … Wilkinson, D. J. (2005). Labelling of anilines, benzylamines and some N-heterocyclics using cycloocta-1,5-dienyliridium(I) -1,1,1,5,5,5-hexafluoro-pentan-2,4-dionate and isotopic hydrogen gas in DMF or DMA. Journal of Labelled Compounds and Radiopharmaceuticals, 48(1), 75–84. https://doi.org/10.1002/jlcr.898
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