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Aerobic addition of secondary phosphine oxides to vinyl sulfides: A shortcut to 1-hydroxy-2-(organosulfanyl)ethyl-(diorganyl)phosphine oxides

Beilstein Journal of Organic Chemistry (2015) 11 1985-1990
DOI: 10.3762/bjoc.11.214
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Abstract

Secondary phosphine oxides react with vinyl sulfides (both alkyl- and aryl-substituted sulfides) under aerobic and solvent-free conditions (80 °C, air, 7-30 h) to afford 1-hydroxy-2-(organosulfanyl)ethyl(diorganyl)phosphine oxides in 70-93% yields.

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Malysheva, S. F., Artem’ev, A. V., Gusarova, N. K., Belogorlova, N. A., Albanov, A. I., Liu, C. W., & Trofimov, B. A. (2015). Aerobic addition of secondary phosphine oxides to vinyl sulfides: A shortcut to 1-hydroxy-2-(organosulfanyl)ethyl-(diorganyl)phosphine oxides. Beilstein Journal of Organic Chemistry, 11, 1985–1990. https://doi.org/10.3762/bjoc.11.214

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