Microwave-assisted synthesis of silver nanoparticles using benzo-18-crown-6 as reducing and stabilizing agent

Abstract

Benzo-18-crown-6 is employed to work as both reducing and stabilizing reagent in the reaction for synthesis of silver nanoparticles. Silver nanoparticles are analyzed using transmission electron microscope and UV–visible spectroscopic technique. The silver nanoparticles prepared in this way are uniform and stable, which can be stored at refrigerator for 5 months. Appearance of surface plasmon band at 420 nm indicated the formation of silver nanoparticles. Highly monodispersed stable silver nanoparticles were obtained within 3 min of microwave irradiation. Through transmission electron microscopy, silver nanoparticles were observed to be spherical.