Abstract
The first electrochemical dehydrogenative C−S bond formation leading to thienoacene derivatives is described. Several thienoacene derivatives were synthesized by dehydrogenative C−H/S−H coupling. The addition of nBu4NBr, which catalytically promoted the reaction as a halogen mediator, was essential.
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APA
Mitsudo, K., Matsuo, R., Yonezawa, T., Inoue, H., Mandai, H., & Suga, S. (2020). Electrochemical Synthesis of Thienoacene Derivatives: Transition-Metal-Free Dehydrogenative C−S Coupling Promoted by a Halogen Mediator. Angewandte Chemie - International Edition, 59(20), 7803–7807. https://doi.org/10.1002/anie.202001149
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