Abstract
The electroreduction of CO32- ions on a molybdenum cathode in a NaCl-KCl-Li2CO3 melt was studied by cyclic voltammetry. The electrochemical synthesis of Mo2C on molybdenum substrates has been performed at 1123 K for 7 h with a cathodic current density of 5 mA cm-2. If molybdenum carbide is present as a thin (ca. 500 nm) film on a molybdenum substrate (Mo2C/Mo), its catalytic activity in the water gas-shift reaction is enhanced by at least an order of magnitude compared to that of the bulk Mo2C phase. © 2014, Verlag der Zeitschrift für Naturforschung. All rights reserved.
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Kuznetsov, S. A., Dubrovskiy, A. R., Rebrov, E. V., & Schouten, J. C. (2007). Electrochemical Synthesis of Mo2C Catalytical Coatings for the Water-Gas Shift Reaction. Zeitschrift Fur Naturforschung - Section A Journal of Physical Sciences, 62(10–11), 647–654. https://doi.org/10.1515/zna-2007-10-1114
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