Journal Article

Synthesis, resolution, and determination of absolute configuration of protected α-ethynylphenylalanine enantiomers

Amino Acids (2015) 47(5) 899-907
DOI: 10.1007/s00726-015-1917-1
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Abstract

Racemic-protected α-ethynylphenylalanine was synthesized from dl-2-benzylserine using α-benzylserinal as key intermediate and was successfully resolved by HPLC on a chiral stationary phase at a semipreparative scale. The absolute configuration of both enantiomers was determined by vibrational circular dichroism.

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Benfodda, Z., Bénimélis, D., Jean, M., Naubron, J. V., Rolland, V., & Meffre, P. (2015). Synthesis, resolution, and determination of absolute configuration of protected α-ethynylphenylalanine enantiomers. Amino Acids, 47(5), 899–907. https://doi.org/10.1007/s00726-015-1917-1

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